全文获取类型
收费全文 | 112246篇 |
免费 | 7947篇 |
国内免费 | 10284篇 |
专业分类
化学 | 48907篇 |
晶体学 | 690篇 |
力学 | 9408篇 |
综合类 | 1630篇 |
数学 | 33291篇 |
物理学 | 36551篇 |
出版年
2023年 | 1248篇 |
2022年 | 1460篇 |
2021年 | 2035篇 |
2020年 | 2291篇 |
2019年 | 2516篇 |
2018年 | 2264篇 |
2017年 | 2719篇 |
2016年 | 3013篇 |
2015年 | 2553篇 |
2014年 | 3883篇 |
2013年 | 7319篇 |
2012年 | 4838篇 |
2011年 | 5315篇 |
2010年 | 4441篇 |
2009年 | 6454篇 |
2008年 | 7052篇 |
2007年 | 7691篇 |
2006年 | 6840篇 |
2005年 | 5662篇 |
2004年 | 5126篇 |
2003年 | 5189篇 |
2002年 | 5237篇 |
2001年 | 3965篇 |
2000年 | 3792篇 |
1999年 | 3312篇 |
1998年 | 3123篇 |
1997年 | 2392篇 |
1996年 | 2150篇 |
1995年 | 2019篇 |
1994年 | 1945篇 |
1993年 | 1585篇 |
1992年 | 1567篇 |
1991年 | 1204篇 |
1990年 | 1025篇 |
1989年 | 865篇 |
1988年 | 764篇 |
1987年 | 631篇 |
1986年 | 545篇 |
1985年 | 574篇 |
1984年 | 577篇 |
1983年 | 298篇 |
1982年 | 458篇 |
1981年 | 510篇 |
1980年 | 366篇 |
1979年 | 362篇 |
1978年 | 282篇 |
1977年 | 260篇 |
1976年 | 180篇 |
1974年 | 130篇 |
1973年 | 129篇 |
排序方式: 共有10000条查询结果,搜索用时 15 毫秒
61.
Nabil N. AL‐Hashimi Rand O. Shahin Aqeel N. AL‐Hashimi Ajeal M. Al Ajeal Lubna H. Tahtamouni Chanbasha Basheer 《Biomedical chromatography : BMC》2019,33(2)
A new cetyl‐alcohol‐reinforced hollow fiber solid/liquid‐phase microextraction (CA–HF–SLPME) followed by high‐performance liquid chromatography–diode array detection (HPLC–DAD) method was developed for simultaneous determination of ezetimibe and simvastatin in human plasma and urine samples. To prepare the CA–HF–SLPME device, the cetyl‐alcohol was immobilized into the pores of a 2.5 cm hollow fiber micro‐tube and the lumen of the micro‐tube was filled with 1‐octanol with the two ends sealed. Afterwards, the prepared device was introduced into 10 mL of the sample solution containing the analytes with agitation. Under optimized conditions, calibration curves plotted in spiked plasma and urine samples were linear in the ranges of 0.363–25/0.49–25 μg L?1 for ezetimibe/simvastatin and 0.193–25/0.312–25 μg L?1 for ezetimibe/simvastatin in plasma and urine samples, respectively. The limit of detection was 0.109/0.174 μg L?1 for ezetimibe/simvastatin in plasma and 0.058/0.093 μg L?1 for ezetimibe/simvastatin in urine. As a potential application, the proposed method was applied to determine the concentration of selected analytes in patient plasma and urine samples after medication and satisfactory results were achieved. In comparison with reference methods, the CA–HF–SLPME–HPLC–DAD method demonstrates considerable potential in the biopharmaceutical analysis of selected drugs. 相似文献
62.
Kozo Matsumoto Tatsuya Miyano Yojiro Kotake 《Journal of polymer science. Part A, Polymer chemistry》2019,57(24):2420-2425
A polycarbosilane having lactose‐derived structures was synthesized, and its thermal property, cytotoxicity, chemical crosslinking, and protein adsorption properties were investigated. The polycarbosilane (PSB‐Lac) was prepared by a thiol‐ene reaction between precursor poly(1‐(3‐butenyl)‐1‐methylsilacyclubane) (PSB) and heptaacetyl lactose that carried a thiol group at the anomeric position, and the successive deprotection of the acetyl groups. The lactose introduction efficiency determined by 1H NMR measurement was 75%. TGA and DSC revealed that the polymer had a 5 wt% decomposition temperature of 260 °C and glass transition temperature (Tg) of 84 °C, which indicated that PSB‐Lac was a thermally stable polymer. PSB‐Lac had no significant cytotoxicity, which was evaluated by human liver cancer cell line HepG2 cultivation on the polystyrene dishes coated with the polymer. Urethane‐crosslinked PSB‐Lac films were prepared by casting solutions of PSB‐Lac and hexamethylene diisocyanate and heating at 120 °C after evaporation of the solvent. The crosslinked PSB‐Lac showed higher adsorption of bovine serum albumin than the similarly crosslinked polycarbosilane that had a glucose structure (PSB‐Glc). © 2019 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2019 , 57, 2420–2425 相似文献
63.
Jamil Chaker 《Mathematische Nachrichten》2019,292(11):2316-2337
We consider systems of stochastic differential equations of the form for with continuous, bounded and non‐degenerate coefficients. Here are independent one‐dimensional stable processes with . In this article we research on uniqueness of weak solutions to such systems by studying the corresponding martingale problem. We prove the uniqueness of weak solutions in the case of diagonal coefficient matrices. 相似文献
64.
Shai Shechter 《Journal of Pure and Applied Algebra》2019,223(10):4384-4425
Let be a complete discrete valuation ring with finite residue field of odd characteristic, and let G be a symplectic or special orthogonal group scheme over . For any let denote the ?-th principal congruence subgroup of . An irreducible character of the group is said to be regular if it is trivial on a subgroup for some ?, and if its restriction to consists of characters of minimal -stabilizer dimension. In the present paper we consider the regular characters of such classical groups over , and construct and enumerate all regular characters of , when the characteristic of is greater than two. As a result, we compute the regular part of their representation zeta function. 相似文献
65.
First, by using linear and trilinear estimates in Bourgain type analytic and Gevrey spaces, the local well‐posedness of the Cauchy problem for the modified Kawahara equation on the line is established for analytic initial data that can be extended as holomorphic functions in a strip around the x‐axis. Next we use this local result and a Gevrey approximate conservation law to prove that global solutions exist. Furthermore, we obtain explicit lower bounds for the radius of spatial analyticity given by , where can be taken arbitrarily small and c is a positive constant. 相似文献
66.
67.
Yasuhito Tanaka 《Operations Research Letters》2019,47(5):406-409
We study a dynamic free-entry oligopoly with sluggish entry and exit of firms under general demand and cost functions. We show that the number of firms in a steady-state open-loop solution for a dynamic free-entry oligopoly is smaller than that at static equilibrium and that the number of firms in a steady-state memoryless closed-loop solution is larger than that in an open-loop solution. 相似文献
68.
《Operations Research Letters》2019,47(3):197-201
The Traveling Salesman Problem with Pickup and Delivery seeks a minimum cost path with pickups preceding deliveries. It is important in on-demand last-mile logistics, such as ride sharing and meal delivery. We examine the use of low-width Decision Diagrams in a branch-and-bound with and without Assignment Problem inference duals as a primal heuristic for finding good solutions within strict time budgets. We show these diagrams can be more effective than similarly structured hybrid Constraint Programming techniques for real-time decision making. 相似文献
69.
Bilender P. Allahverdiev 《Mathematical Methods in the Applied Sciences》2019,42(1):229-236
In this study, maximal dissipative second‐order dynamic operators on semi‐infinite time scale are studied in the Hilbert space , that the extensions of a minimal symmetric operator in limit‐point case. We construct a self‐adjoint dilation of the dissipative operator together with its incoming and outgoing spectral representations so that we can determine the scattering function of the dilation as stated in the scheme of Lax‐Phillips. Moreover, we construct a functional model of the dissipative operator and identify its characteristic function in terms of the Weyl‐Titchmarsh function of a self‐adjoint second‐order dynamic operator. Finally, we prove the theorems on completeness of the system of root functions of the dissipative and accumulative dynamic operators. 相似文献
70.
Awatif Alqahtani Mohamed Jleli Bessem Samet 《Mathematical Methods in the Applied Sciences》2019,42(3):861-870
In this paper, some nonlocal in time differential inequalities of Sobolev type are considered. Using the nonlinear capacity method, sufficient conditions for the nonexistence of nontrivial global classical solutions are provided. 相似文献